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undergraduate thesis
Mehanokemijska sinteza kalcijeva oksalata
2018. urn:nbn:hr:182:889306
Sekulić, Marina
Josip Juraj Strossmayer University of Osijek
Department of Chemistry
Department of General, Inorganic and Physical Chemistry and Methodology of Chemistry

Cite this document

Sekulić, M. (2018). Mehanokemijska sinteza kalcijeva oksalata (Undergraduate thesis). Retrieved from https://urn.nsk.hr/urn:nbn:hr:182:889306

Sekulić, Marina. "Mehanokemijska sinteza kalcijeva oksalata." Undergraduate thesis, Josip Juraj Strossmayer University of Osijek, Department of Chemistry, 2018. https://urn.nsk.hr/urn:nbn:hr:182:889306

Sekulić, Marina. "Mehanokemijska sinteza kalcijeva oksalata." Undergraduate thesis, Josip Juraj Strossmayer University of Osijek, Department of Chemistry, 2018. https://urn.nsk.hr/urn:nbn:hr:182:889306

Sekulić, M. (2018). 'Mehanokemijska sinteza kalcijeva oksalata', Undergraduate thesis, Josip Juraj Strossmayer University of Osijek, Department of Chemistry, accessed 15 March 2023, https://urn.nsk.hr/urn:nbn:hr:182:889306

Sekulić M. Mehanokemijska sinteza kalcijeva oksalata [Undergraduate thesis]. Osijek: Josip Juraj Strossmayer University of Osijek, Department of Chemistry; 2018 [cited 2023 March 15] Available at: https://urn.nsk.hr/urn:nbn:hr:182:889306

M. Sekulić, "Mehanokemijska sinteza kalcijeva oksalata", Undergraduate thesis, Josip Juraj Strossmayer University of Osijek, Department of Chemistry, Osijek, 2018. Available at: https://urn.nsk.hr/urn:nbn:hr:182:889306

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Metadata
TitleMehanokemijska sinteza kalcijeva oksalata
Title (english)The mechanochemical synthesis of calcium oxalate
AuthorMarina Sekulić
MentorIgor Đerđ (mentor)
MentorAnamarija Stanković (pomoć pri izradi, neposredni voditelj)
GranterJosip Juraj Strossmayer University of Osijek
Department of Chemistry
(Department of General, Inorganic and Physical Chemistry and Methodology of Chemistry)
Osijek
Defense date and country2018-09-11, Croatia
Scientific / art field,
discipline and subdiscipline		NATURAL SCIENCES
Chemistry
Inorganic Chemistry
Abstract
Ova studija prikazuje mehanokemijsku sintezu kalcijeva oksalata u planetarnom kugličnom mlinu, bez i uz prisutnost otapala. Dosadašnja istraživanja su uglavnom bila usmjerena na otopinsku sintezu kalcijeva oksalata. U ovom radu opisujemo drugačiji pristup, koji će donijeti nova saznanja o sintezi kristala kalcijeva oksalata, a koje su uzrokovane utjecajem mehaničke energije. Cilj istraživanja je sinteza, identifikacija i karakterizacija pojedine oksalatne hidratne faze sintetizirane iz kalcijevih soli (klorida, nitrata i sulfata). Ispitivan je utjecaj brzine mljevenja i praćena je reakcija u ovisnosti o vremenu sinteze. Strukturalna i termička svojstva uzoraka ispitana su FTIR spektroskopijom i termogravimetrijskom analizom (TGA). Morfološke karakteristike kalcijeva oksalata te raspodjela veličine čestica određene su optičkom mikroskopijom i dinamičkim raspršenjem svjetlosti (DLS).
Abstract (english)
In this work, mechanochemical synthesis of calcium oxalate was done in planetary ball mill, with and without addition of water as a solvent. Previous researches were primarily focused on calcium oxalate synthesis in a solution. Here we report a different approach which may contribute to new findings in calcium oxalate crystal synthesis caused by an influence of mechanical energy. The aim of this study is synthesis, identification and characterization of particular oxalate hydrate phase synthesized with calcium salts (chloride, nitrate and sulphate). The effects of grinding speed and reaction duration regarding the time of synthesis were investigated. Structural and thermal sample properties were studied by FTIR spectroscopy and thermogravimetric analysis (TGA). Morphologic characteristics of calcium oxalate and size distribution were measured by optical microscopy and dynamic light scattering (DLS).
Keywords
Keywords (english)
Languagecroatian
URN:NBNurn:nbn:hr:182:889306
Study programmeTitle: Chemistry
Study programme type: university
Study level: undergraduate
Academic / professional title: sveučilišni/a prvostupnik/prvostupnica (baccalaureus/baccalaurea) kemije (sveučilišni/a prvostupnik/prvostupnica (baccalaureus/baccalaurea) kemije)
Type of resourceText
File originBorn digital
Access conditionsOpen access
Terms of useLicence In copyright icon
Created on2018-12-17 11:50:50