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master's thesis
Mehanokemijska sinteza metalnih kompleksa sa Schiffovim bazama
2019. urn:nbn:hr:182:444549
Szep, Ivana
Josip Juraj Strossmayer University of Osijek
Department of Chemistry
Department of General, Inorganic and Physical Chemistry and Methodology of Chemistry

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Szep, I. (2019). Mehanokemijska sinteza metalnih kompleksa sa Schiffovim bazama (Master's thesis). Osijek: Josip Juraj Strossmayer University of Osijek, Department of Chemistry. Retrieved from https://urn.nsk.hr/urn:nbn:hr:182:444549

Szep, Ivana. "Mehanokemijska sinteza metalnih kompleksa sa Schiffovim bazama." Master's thesis, Josip Juraj Strossmayer University of Osijek, Department of Chemistry, 2019. https://urn.nsk.hr/urn:nbn:hr:182:444549

Szep, Ivana. "Mehanokemijska sinteza metalnih kompleksa sa Schiffovim bazama." Master's thesis, Josip Juraj Strossmayer University of Osijek, Department of Chemistry, 2019. https://urn.nsk.hr/urn:nbn:hr:182:444549

Szep, I. (2019). 'Mehanokemijska sinteza metalnih kompleksa sa Schiffovim bazama', Master's thesis, Josip Juraj Strossmayer University of Osijek, Department of Chemistry, accessed 16 November 2024, https://urn.nsk.hr/urn:nbn:hr:182:444549

Szep I. Mehanokemijska sinteza metalnih kompleksa sa Schiffovim bazama [Master's thesis]. Osijek: Josip Juraj Strossmayer University of Osijek, Department of Chemistry; 2019 [cited 2024 November 16] Available at: https://urn.nsk.hr/urn:nbn:hr:182:444549

I. Szep, "Mehanokemijska sinteza metalnih kompleksa sa Schiffovim bazama", Master's thesis, Josip Juraj Strossmayer University of Osijek, Department of Chemistry, Osijek, 2019. Available at: https://urn.nsk.hr/urn:nbn:hr:182:444549

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Metadata
TitleMehanokemijska sinteza metalnih kompleksa sa Schiffovim bazama
Title (english)Mchanochemical syntesis of metal complexes with Schiffs bases
AuthorIvana Szep
MentorElvira Kovač-Andrić (mentor)
Committee memberTomislav Balić (predsjednik povjerenstva)
Committee memberElvira Kovač-Andrić (član povjerenstva)
Committee memberBrunislav Matasović (član povjerenstva)
GranterJosip Juraj Strossmayer University of Osijek
Department of Chemistry
(Department of General, Inorganic and Physical Chemistry and Methodology of Chemistry)
Osijek
Defense date and country2019-09-17, Croatia
Scientific / art field,
discipline and subdiscipline		NATURAL SCIENCES
Chemistry
Inorganic Chemistry
Abstract
Mehanokemijske sinteze se u današnje vrijeme sve više proučavaju i proširuju zbog toga što omogućavaju nekorištenje otapala (ili pak uporabu minimalne količine otapala), kraće vrijeme sinteze te veće iskorištenje. U ovom diplomskom radu sintetizirani su metalni kompleksi metalnih soli sa Schiffovim bazama metodom visokoenergetskog mljevenja unutar planetarnog kugličnog mlina te su uspoređeni s produktima dobivenim klasičnom sintezom. Dobiveni spojevi okarakterizirani su termogravimatrijskom analizom (TGA), infracrvenom spektroskopijom (FT-IR) i elementnom analizom (CHN). Uz to, mijenjani su promjenjivi parametri kao što su vrijeme sinteze te brzina okretaja kako bi se dobili što točniji uvjeti nastajanja željenih spojeva.
Abstract (english)
Mechanochemical synthesis are being explored and expanded because they allow minimal usability of soluble reactants, or don't use any of it, shorter synthesis time and they are more effective. In this graduate thesis, metal complexes of metal salts with Schiff's bases are synthesized by the method of high-energy grinding within a planetary ball mill and are compared to products of classic synthesis. The obtained compounds are characterized by thermogravimetric analysis (TGA), Fourier transform infrared spectroscopy (FT-IR) and elemental analyses (CHN). On the other hand, variable parameters like reaction time and rotation speed, are changed in order to obtain the most accurate conditions of the desired compounds.
Keywords
Keywords (english)
Languagecroatian
URN:NBNurn:nbn:hr:182:444549
Study programmeTitle: Chemistry
Study programme type: university
Study level: graduate
Academic / professional title: magistar/magistra edukacije kemije (magistar/magistra edukacije kemije)
Type of resourceText
File originBorn digital
Access conditionsOpen access
Terms of useLicence In copyright icon
Created on2019-11-20 08:43:59