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undergraduate thesis
Priprava estera piridinona s meta-supstituiranim arilom i cimetne kiseline
2019. urn:nbn:hr:182:121322
Vladika, Marija
Josip Juraj Strossmayer University of Osijek
Department of Chemistry
Department of Analytical, Organic and Applied Chemistry

Cite this document

Vladika, M. (2019). Priprava estera piridinona s meta-supstituiranim arilom i cimetne kiseline (Undergraduate thesis). Osijek: Josip Juraj Strossmayer University of Osijek, Department of Chemistry. Retrieved from https://urn.nsk.hr/urn:nbn:hr:182:121322

Vladika, Marija. "Priprava estera piridinona s meta-supstituiranim arilom i cimetne kiseline." Undergraduate thesis, Josip Juraj Strossmayer University of Osijek, Department of Chemistry, 2019. https://urn.nsk.hr/urn:nbn:hr:182:121322

Vladika, Marija. "Priprava estera piridinona s meta-supstituiranim arilom i cimetne kiseline." Undergraduate thesis, Josip Juraj Strossmayer University of Osijek, Department of Chemistry, 2019. https://urn.nsk.hr/urn:nbn:hr:182:121322

Vladika, M. (2019). 'Priprava estera piridinona s meta-supstituiranim arilom i cimetne kiseline', Undergraduate thesis, Josip Juraj Strossmayer University of Osijek, Department of Chemistry, accessed 19 April 2024, https://urn.nsk.hr/urn:nbn:hr:182:121322

Vladika M. Priprava estera piridinona s meta-supstituiranim arilom i cimetne kiseline [Undergraduate thesis]. Osijek: Josip Juraj Strossmayer University of Osijek, Department of Chemistry; 2019 [cited 2024 April 19] Available at: https://urn.nsk.hr/urn:nbn:hr:182:121322

M. Vladika, "Priprava estera piridinona s meta-supstituiranim arilom i cimetne kiseline", Undergraduate thesis, Josip Juraj Strossmayer University of Osijek, Department of Chemistry, Osijek, 2019. Available at: https://urn.nsk.hr/urn:nbn:hr:182:121322

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Metadata
TitlePriprava estera piridinona s meta-supstituiranim arilom i cimetne kiseline
Title (english)Preparation of cinnamic acid esters with pyridinones containing meta substitudet aryl
AuthorMarija Vladika
MentorAleksandar Sečenji (mentor)
MentorAndrea Dandić (pomoć pri izradi, neposredni voditelj)
GranterJosip Juraj Strossmayer University of Osijek
Department of Chemistry
(Department of Analytical, Organic and Applied Chemistry)
Osijek
Defense date and country2019-09-16, Croatia
Scientific / art field,
discipline and subdiscipline		NATURAL SCIENCES
Chemistry
Organic Chemistry
Abstract
U ovom završnom radu opisana je priprava estera meta-supstituiranih N-aril-3-hidroksipiridin-4-ona. Za esterifikaciju N-aril-3-hidroksipiridin-4-ona korištena je cimetna kiselina koja je uvedena metodom Steglichove esterifikacije. Meta supstituirani N-aril-3-hidroksipiridin-4-oni pripravljeni su direktnom metodom iz 3-hidroksi-2-metilpiran-4-ona (maltol) i meta supstituiranih anilina, uz upotrebu p-toluensulfonske kiseline (p-TsOH) kao kiselog katalizatora, u autoklavu. Pripravljeni meta supstituirani derivati N-aril-3-hidroksipiridin-4-ona poslužili su kao polazni spojevi za sintezu njihovih esterskih derivata s cimetnom kiselinom [2-metil-1-(m-metoksifenil)piridin-4-on-3-il]-3-fenilprop-2-enoata (spoj 3) i [2-metil-1-(m-metilfenil)piridin-4-on-3-il]-3-fenilprop-2-enoata (spoj 4).
Abstract (english)
In this work the preparation of meta substituted N-aryl-3-hydroxypyridin-4-one esters is described. For esterification of N-aryl-3-hydroxypyridin-4-one cinnamic acid is used which was introduced by Steglich esterification method. The meta substituted N-aryl-3-hydroxypyridin-4-ones were prepared by direct method from 3-hydroxy-2-methylpyran-4-one (maltol) and meta substituted anilines, using p-toluenesulfonic acid (p-TsOH) as acidic catalyst, in autoclave. Prepared meta substituted derivatives of N-aryl-3-hydroxypyridine-4-ones were used as starting compounds for the synthesis of ester derivates of cinnamic acid [2-methyl-1- (m-methoxyphenyl) pyridin-4-one-3-yl] -3-phenylprop-2-enoate (compound 3) and [2-methyl-1- (m-methylphenyl) pyridin-4-on-3-yl] -3-phenylprop-2-enoate (compound 4).
Keywords
Keywords (english)
Languagecroatian
URN:NBNurn:nbn:hr:182:121322
Study programmeTitle: Chemistry
Study programme type: university
Study level: undergraduate
Academic / professional title: sveučilišni/a prvostupnik/prvostupnica (baccalaureus/baccalaurea) kemije (sveučilišni/a prvostupnik/prvostupnica (baccalaureus/baccalaurea) kemije)
Type of resourceText
File originBorn digital
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Created on2019-12-06 10:47:27