prikaz prve stranice dokumenta Priprava estera cimetne kiseline s meta- i para-nitro derivatima N-arilpiridinona
  Download
PDF 720.64 KB
undergraduate thesis
Priprava estera cimetne kiseline s meta- i para-nitro derivatima N-arilpiridinona
2018. urn:nbn:hr:182:029547
Šoltić, Monika
Josip Juraj Strossmayer University of Osijek
Department of Chemistry
Department of Analytical, Organic and Applied Chemistry

Cite this document

Šoltić, M. (2018). Priprava estera cimetne kiseline s meta- i para-nitro derivatima N-arilpiridinona (Undergraduate thesis). Osijek: Josip Juraj Strossmayer University of Osijek, Department of Chemistry. Retrieved from https://urn.nsk.hr/urn:nbn:hr:182:029547

Šoltić, Monika. "Priprava estera cimetne kiseline s meta- i para-nitro derivatima N-arilpiridinona." Undergraduate thesis, Josip Juraj Strossmayer University of Osijek, Department of Chemistry, 2018. https://urn.nsk.hr/urn:nbn:hr:182:029547

Šoltić, Monika. "Priprava estera cimetne kiseline s meta- i para-nitro derivatima N-arilpiridinona." Undergraduate thesis, Josip Juraj Strossmayer University of Osijek, Department of Chemistry, 2018. https://urn.nsk.hr/urn:nbn:hr:182:029547

Šoltić, M. (2018). 'Priprava estera cimetne kiseline s meta- i para-nitro derivatima N-arilpiridinona', Undergraduate thesis, Josip Juraj Strossmayer University of Osijek, Department of Chemistry, accessed 09 November 2024, https://urn.nsk.hr/urn:nbn:hr:182:029547

Šoltić M. Priprava estera cimetne kiseline s meta- i para-nitro derivatima N-arilpiridinona [Undergraduate thesis]. Osijek: Josip Juraj Strossmayer University of Osijek, Department of Chemistry; 2018 [cited 2024 November 09] Available at: https://urn.nsk.hr/urn:nbn:hr:182:029547

M. Šoltić, "Priprava estera cimetne kiseline s meta- i para-nitro derivatima N-arilpiridinona", Undergraduate thesis, Josip Juraj Strossmayer University of Osijek, Department of Chemistry, Osijek, 2018. Available at: https://urn.nsk.hr/urn:nbn:hr:182:029547

Please login to the repository to save this object to your list.
Metadata
TitlePriprava estera cimetne kiseline s meta- i para-nitro derivatima N-arilpiridinona
Title (english)Preparation of cinnamic acid ester with meta and para nitro derivatives of N-aryl pyridinones
AuthorMonika Šoltić
MentorAleksandar Sečenji (mentor)
MentorAndrea Dandić (pomoć pri izradi, neposredni voditelj)
GranterJosip Juraj Strossmayer University of Osijek
Department of Chemistry
(Department of Analytical, Organic and Applied Chemistry)
Osijek
Defense date and country2018-09-20, Croatia
Scientific / art field,
discipline and subdiscipline		NATURAL SCIENCES
Chemistry
Organic Chemistry
Abstract
U ovome završnom radu opisana je sinteza estera cimetne kiseline s meta- i para-nitro derivatima N-arilpiridinona. U prvome djelu opisana je priprava N-aril supstituiranih 3-hidroksipiridin-4-ona, spoja 1 (3-hidroksi-2-metil-1-(m-nitrofenil)piridin-4-on) i spoja 2 (3-hidroksi-2-metil-1-(p-nitrofenil)piridin-4-on). Spojevi 1 i 2 pripravljeni direktnom metodom iz maltola i određenog primarnog amina, korišteni su u drugome djelu rada kao polazni spojevi u sintezi spojeva 3 ([2-metil-1-(m-nitrofenil)piridin-4-on-3-il]-3-fenilprop-2-enoata) i 4 ([2-metil-1-(p-nitrofenil)piridin-4-on-3-il]-3-fenilprop-2-enoata). Oba esterska derivata 3,4-HP i cimetne kiseline uspješno su pripravljena Steglichovom metodom esterifikacije. Strukture sintetiziranih spojeva potvrđene su NMR spektroskopijom (\(^{1}H \),\(^{13}C \) , DEPTQ).
Abstract (english)
In this work preparation of cinnamic acid derivatives of N-arylpyridinones is described. In the first part of this work preparation of N-aryl substituted 3-hydroxypyridin-4-ones, compound 1 (3-hydroxy-2-methyl-1-(m-nitrophenyl)pyridin-4-one) and compound 2 (3-hydroxy-2-methyl-1-(p-nitrophenyl)pyridin-4one) is presented. These two compounds were prepared from maltol and primary amine using direct method. In the second part of this work prepared compounds (1 and 2) were used as starting compounds in the synthesis of compounds 3 ([2-methyl-1-(m-nitrophenyl)pyridin-4-on-3-yl]-3-phenylprop-2-enoate) and 4 ([2-methyl-1-(p-nitrophenyl)pyridin-4-on-3-yl]-3-phenylprop-2-enoate). For esterification of compounds 1 and 2 with cinnamic acid Steglich esterification method was used. The structures of synthesized compounds were identified by NMR spectroscopy (\(^{1}H \),\(^{13}C\) , DEPTQ).
Keywords
Keywords (english)
Languagecroatian
URN:NBNurn:nbn:hr:182:029547
Study programmeTitle: Chemistry
Study programme type: university
Study level: undergraduate
Academic / professional title: sveučilišni/a prvostupnik/prvostupnica (baccalaureus/baccalaurea) kemije (sveučilišni/a prvostupnik/prvostupnica (baccalaureus/baccalaurea) kemije)
Type of resourceText
File originBorn digital
Access conditionsOpen access
Terms of useLicence In copyright icon
Created on2018-12-17 09:56:03