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master's thesis
Rješavanje i utočnjavanje kristalnih struktura spojeva s inkludiranim plinovima
2021. urn:nbn:hr:182:506151
Vladika, Marija
Josip Juraj Strossmayer University of Osijek
Department of Chemistry
Department of General, Inorganic and Physical Chemistry and Methodology of Chemistry

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Vladika, M. (2021). Rješavanje i utočnjavanje kristalnih struktura spojeva s inkludiranim plinovima (Master's thesis). Retrieved from https://urn.nsk.hr/urn:nbn:hr:182:506151

Vladika, Marija. "Rješavanje i utočnjavanje kristalnih struktura spojeva s inkludiranim plinovima." Master's thesis, Josip Juraj Strossmayer University of Osijek, Department of Chemistry, 2021. https://urn.nsk.hr/urn:nbn:hr:182:506151

Vladika, Marija. "Rješavanje i utočnjavanje kristalnih struktura spojeva s inkludiranim plinovima." Master's thesis, Josip Juraj Strossmayer University of Osijek, Department of Chemistry, 2021. https://urn.nsk.hr/urn:nbn:hr:182:506151

Vladika, M. (2021). 'Rješavanje i utočnjavanje kristalnih struktura spojeva s inkludiranim plinovima', Master's thesis, Josip Juraj Strossmayer University of Osijek, Department of Chemistry, accessed 15 March 2023, https://urn.nsk.hr/urn:nbn:hr:182:506151

Vladika M. Rješavanje i utočnjavanje kristalnih struktura spojeva s inkludiranim plinovima [Master's thesis]. Osijek: Josip Juraj Strossmayer University of Osijek, Department of Chemistry; 2021 [cited 2023 March 15] Available at: https://urn.nsk.hr/urn:nbn:hr:182:506151

M. Vladika, "Rješavanje i utočnjavanje kristalnih struktura spojeva s inkludiranim plinovima", Master's thesis, Josip Juraj Strossmayer University of Osijek, Department of Chemistry, Osijek, 2021. Available at: https://urn.nsk.hr/urn:nbn:hr:182:506151

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Metadata
TitleRješavanje i utočnjavanje kristalnih struktura spojeva s inkludiranim plinovima
Title (english)Crystal structure solution and refinement of compounds with included gases
AuthorMarija Vladika
MentorTomislav Balić (mentor)
Committee memberAnamarija Stanković (predsjednik povjerenstva)
Committee memberTomislav Balić (član povjerenstva)
Committee memberMartina Medvidović-Kosanović (član povjerenstva)
GranterJosip Juraj Strossmayer University of Osijek
Department of Chemistry
(Department of General, Inorganic and Physical Chemistry and Methodology of Chemistry)
Osijek
Defense date and country2021-12-07, Croatia
Scientific / art field,
discipline and subdiscipline		NATURAL SCIENCES
Chemistry
Inorganic Chemistry
Abstract
Makrociklička Schiffova baza N4O4 (1,6,20,25-tetraaza2,5: 8,9: 17,18: 21,24: 27,28: 36,37-heksabenzo-10,16,29,35-tetraoksa-ciklooktatriakonta-1,6,20,25-tetraen)(1) pripravljena je reakcijom [2 + 2] ciklokondenzacije odgovarajućeg dialdehida i diamina. Kristalna i molekulska struktura određena je rendgenskom difrakcijom na monokristalnom uzorku spoja. Predmet ovog rada je rješavanje i utočnjavanje kristalnih struktura 5 zadanih makrocikličkih spojeva (1xCO2, 1xNH3, 1xCl2, 1xSO2, 1xH2S) pripravljenih izlaganjem kloroformskog solvata (1xCLF) parama CO2, NH3, Cl2, SO2, i H2S. Za utočnjavanje i rješavanje kristalnih struktura korišteni su programi Olex2 i Mercury. Spojevima je određena struktura i kristalografski parametri.
Abstract (english)
Macrocyclic Schiff base N4O4 (1,6,20,25-tetraaza2,5: 8,9: 17,18: 21,24: 27,28: 36,37-hexabenzo-10,16,29,35-tetraoxa-cyclooctatriaconta -1,6,20,25-tetraene) (1) was prepared by the [2 + 2] cyclocondensation reaction of the corresponding dialdehyde and diamine. The crystal and molecular structure was determined by X-ray diffraction on a single crystal sample of the compound. The subject of this paper is solving and refining the crystal structures of 5 given macrocyclic compounds (1xCO2, 1xNH3, 1xCl2, 1xSO2, 1xH2S) prepared by exposing chloroform solvate (1xCLF) to CO2, NH3, Cl2, SO2, and H2S vapors. Olex2 and Mercury programs were used to refine and resolve crystal structures. The structure and crystallographic parameters were determined by the compounds.
Keywords
Keywords (english)
Languagecroatian
URN:NBNurn:nbn:hr:182:506151
Study programmeTitle: Graduate University Study of Chemistry; research program; specializations in: Research program
Course: Research program
Study programme type: university
Study level: graduate
Academic / professional title: magistar/magistra kemije (magistar/magistra kemije)
Type of resourceText
File originBorn digital
Access conditionsOpen access
Terms of useLicence In copyright icon
Created on2022-08-02 09:16:30