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master's thesis
Sinteza pendantnih makrocikličkih spojeva reakcijama N-alkiliranja makrocikličkih amina
2024. urn:nbn:hr:182:878013
Jozić, Rajna Marija
Josip Juraj Strossmayer University of Osijek
Department of Chemistry
Department of Analytical, Organic and Applied Chemistry

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Jozić, R. M. (2024). Sinteza pendantnih makrocikličkih spojeva reakcijama N-alkiliranja makrocikličkih amina (Master's thesis). Osijek: Josip Juraj Strossmayer University of Osijek, Department of Chemistry. Retrieved from https://urn.nsk.hr/urn:nbn:hr:182:878013

Jozić, Rajna Marija. "Sinteza pendantnih makrocikličkih spojeva reakcijama N-alkiliranja makrocikličkih amina." Master's thesis, Josip Juraj Strossmayer University of Osijek, Department of Chemistry, 2024. https://urn.nsk.hr/urn:nbn:hr:182:878013

Jozić, Rajna Marija. "Sinteza pendantnih makrocikličkih spojeva reakcijama N-alkiliranja makrocikličkih amina." Master's thesis, Josip Juraj Strossmayer University of Osijek, Department of Chemistry, 2024. https://urn.nsk.hr/urn:nbn:hr:182:878013

Jozić, R. M. (2024). 'Sinteza pendantnih makrocikličkih spojeva reakcijama N-alkiliranja makrocikličkih amina', Master's thesis, Josip Juraj Strossmayer University of Osijek, Department of Chemistry, accessed 28 October 2024, https://urn.nsk.hr/urn:nbn:hr:182:878013

Jozić RM. Sinteza pendantnih makrocikličkih spojeva reakcijama N-alkiliranja makrocikličkih amina [Master's thesis]. Osijek: Josip Juraj Strossmayer University of Osijek, Department of Chemistry; 2024 [cited 2024 October 28] Available at: https://urn.nsk.hr/urn:nbn:hr:182:878013

R. M. Jozić, "Sinteza pendantnih makrocikličkih spojeva reakcijama N-alkiliranja makrocikličkih amina", Master's thesis, Josip Juraj Strossmayer University of Osijek, Department of Chemistry, Osijek, 2024. Available at: https://urn.nsk.hr/urn:nbn:hr:182:878013

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Metadata
TitleSinteza pendantnih makrocikličkih spojeva reakcijama N-alkiliranja makrocikličkih amina
Title (english)Synthesis of pendant macrocycles by N-alkylation reactions on amine macrocycles
AuthorRajna Marija Jozić
MentorTomislav Balić (mentor)
Committee memberMartina Medvidović-Kosanović (predsjednik povjerenstva)
Committee memberTomislav Balić (član povjerenstva)
Committee memberAleksandar Sečenji (član povjerenstva)
GranterJosip Juraj Strossmayer University of Osijek
Department of Chemistry
(Department of Analytical, Organic and Applied Chemistry)
Osijek
Defense date and country2024-09-20, Croatia
Scientific / art field,
discipline and subdiscipline		NATURAL SCIENCES
Chemistry
Organic Chemistry
Abstract
Cilj ovog diplomskog rada je sinteza pendantnih makrocikli kih spojeva reakcijama N-alkiliranja makrocikli kih amina. Makrocikli ka Schiffova baza, pripremljena iz dialdehida i diamina, reducirana je natrijevim borohidridom. Reducirani je oblik potom metiliran, a sredstva za metiliranje su bili metil-4-(bromometil)benzoat i metil bromoacetat. Tijek svake reakcije metilacije je pra en tankoslojnom kromatografijom. Spojevi su karakterizirani IR (FTIR) i 1H NMR spektroskopijom. Iz izvedenih sinteza, uspjebno su dobivena i identificirana dva nova pendantna makrocikli ka spoja.
Abstract (english)
The aim of this thesis was the synthesis of pendant macrocyclic compounds via Nalkylation reactions of macrocyclic amines. The macrocyclic Schiff base, prepared from a dialdehyde and diamine, was reduced using sodium borohydride. The reduced form was methylated using methyl-4-(bromomethyl) benzoate and methyl bromoacetate. The progress of each methylation reaction was monitored by thin-layer chromatography. Two novel pendant macrocycles were successfully obtained and characterized using IR (FT-IR) and ¹H NMR spectroscopy.
Keywords
Keywords (english)
Languagecroatian
URN:NBNurn:nbn:hr:182:878013
Study programmeTitle: University Graduate Study of Chemistry; Research Program; specializations in: Research Program
Course: Research Program
Study programme type: university
Study level: graduate
Academic / professional title: sveučilišni/a magistar/magistra kemije (sveučilišni/a magistar/magistra kemije)
Type of resourceText
File originBorn digital
Access conditionsOpen access
Terms of useLicence In copyright icon
Created on2024-10-07 06:57:15