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undergraduate thesis
Mehanokemijska sinteza kalcijeva oksalata iz kalcijeva nitrata
2018. urn:nbn:hr:182:499981
Goman, Dominik
Josip Juraj Strossmayer University of Osijek
Department of Chemistry
Department of General, Inorganic and Physical Chemistry and Methodology of Chemistry

Cite this document

Goman, D. (2018). Mehanokemijska sinteza kalcijeva oksalata iz kalcijeva nitrata (Undergraduate thesis). Osijek: Josip Juraj Strossmayer University of Osijek, Department of Chemistry. Retrieved from https://urn.nsk.hr/urn:nbn:hr:182:499981

Goman, Dominik. "Mehanokemijska sinteza kalcijeva oksalata iz kalcijeva nitrata." Undergraduate thesis, Josip Juraj Strossmayer University of Osijek, Department of Chemistry, 2018. https://urn.nsk.hr/urn:nbn:hr:182:499981

Goman, Dominik. "Mehanokemijska sinteza kalcijeva oksalata iz kalcijeva nitrata." Undergraduate thesis, Josip Juraj Strossmayer University of Osijek, Department of Chemistry, 2018. https://urn.nsk.hr/urn:nbn:hr:182:499981

Goman, D. (2018). 'Mehanokemijska sinteza kalcijeva oksalata iz kalcijeva nitrata', Undergraduate thesis, Josip Juraj Strossmayer University of Osijek, Department of Chemistry, accessed 07 December 2024, https://urn.nsk.hr/urn:nbn:hr:182:499981

Goman D. Mehanokemijska sinteza kalcijeva oksalata iz kalcijeva nitrata [Undergraduate thesis]. Osijek: Josip Juraj Strossmayer University of Osijek, Department of Chemistry; 2018 [cited 2024 December 07] Available at: https://urn.nsk.hr/urn:nbn:hr:182:499981

D. Goman, "Mehanokemijska sinteza kalcijeva oksalata iz kalcijeva nitrata", Undergraduate thesis, Josip Juraj Strossmayer University of Osijek, Department of Chemistry, Osijek, 2018. Available at: https://urn.nsk.hr/urn:nbn:hr:182:499981

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Metadata
TitleMehanokemijska sinteza kalcijeva oksalata iz kalcijeva nitrata
Title (english)Mehanochemical synthesis of calcium oxalate from calcium nitrate
AuthorDominik Goman
MentorIgor Đerđ (mentor)
MentorAnamarija Stanković (pomoć pri izradi, neposredni voditelj)
GranterJosip Juraj Strossmayer University of Osijek
Department of Chemistry
(Department of General, Inorganic and Physical Chemistry and Methodology of Chemistry)
Osijek
Defense date and country2018-09-21, Croatia
Scientific / art field,
discipline and subdiscipline		NATURAL SCIENCES
Chemistry
Inorganic Chemistry
Abstract
Ovim istraživanjem je prikazana mehanokemijska sinteza kalcijeva oksalata, bez i uz prisutnost otapala (vode), u planetarnom kugličnom mlinu. Sva istraživanja do sada su ponajviše bila usmjerena na sintezu kalcijeva oksalata otopinskom kemijom. Ovim radom nastojalo se opisati drugačiji pristup, kako bi se pridonijelo novim saznanjima o sintezi kalcijeva oksalata, ekološki osvještenijom, mehanokemijskom metodom. Konačni cilj istraživanja jest sinteza, karakterizacija te identifikacija pojedine hidratne faze, dobivene reakcijom kalcijeva nitrata tetrahidrata i natrijeva oksalata. Reakcija je praćena u ovisnosti o vremenu reakcije i brzini mljevenja. Strukturna i termička svojstva uzoraka ispitana su FT-IR spektroskopijom i termogravimetrijskom analizom (TGA). Morfološke osobine kalcijeva oksalata, kao i klasifikacija veličine čestica, određene su optičkom mikroskopijom i metodom dinamičkog raspršenja svjetlosti (DLS).
Abstract (english)
The study presents the mechanochemical synthesis of calcium oxalate, without and in the presence of solvents, in a planetary ball mill. All studies so far have focused mainly on the synthesis of calcium oxalate using solution chemistry. In this paper, we described a different approach that could contribute to new findings in the field of calcium oxalate synthesis using mechanochemical approach. The ultimate goal of the research is synthesis, as well as structural characterization and identification of individual oxalate hydrate phase, gained by the synthesis of calcium salts (of the chlorides, nitrates and sulphates). The reaction is monitored depending on the duration of the synthesis, to determine if the effect of the milling velocity on the reaction exists. Structural and thermal properties of the sample were tested by FTIR spectroscopy and thermogravimetric analysis (TGA). Morphological properties of calcium oxalate as well as particle size distribution are gained by optical microscopy and dynamic light scattering (DLS).
Keywords
Keywords (english)
Languagecroatian
URN:NBNurn:nbn:hr:182:499981
Study programmeTitle: Chemistry
Study programme type: university
Study level: undergraduate
Academic / professional title: sveučilišni/a prvostupnik/prvostupnica (baccalaureus/baccalaurea) kemije (sveučilišni/a prvostupnik/prvostupnica (baccalaureus/baccalaurea) kemije)
Type of resourceText
File originBorn digital
Access conditionsOpen access
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Created on2018-12-17 10:15:49