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undergraduate thesis
Mehanokemijska sinteza kompleksa prijelaznih metala u zeolitima
2022. urn:nbn:hr:182:722405
Šinjori, Damjan
Josip Juraj Strossmayer University of Osijek
Department of Chemistry
Department of General, Inorganic and Physical Chemistry and Methodology of Chemistry

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Šinjori, D. (2022). Mehanokemijska sinteza kompleksa prijelaznih metala u zeolitima (Undergraduate thesis). Osijek: Josip Juraj Strossmayer University of Osijek, Department of Chemistry. Retrieved from https://urn.nsk.hr/urn:nbn:hr:182:722405

Šinjori, Damjan. "Mehanokemijska sinteza kompleksa prijelaznih metala u zeolitima." Undergraduate thesis, Josip Juraj Strossmayer University of Osijek, Department of Chemistry, 2022. https://urn.nsk.hr/urn:nbn:hr:182:722405

Šinjori, Damjan. "Mehanokemijska sinteza kompleksa prijelaznih metala u zeolitima." Undergraduate thesis, Josip Juraj Strossmayer University of Osijek, Department of Chemistry, 2022. https://urn.nsk.hr/urn:nbn:hr:182:722405

Šinjori, D. (2022). 'Mehanokemijska sinteza kompleksa prijelaznih metala u zeolitima', Undergraduate thesis, Josip Juraj Strossmayer University of Osijek, Department of Chemistry, accessed 13 February 2025, https://urn.nsk.hr/urn:nbn:hr:182:722405

Šinjori D. Mehanokemijska sinteza kompleksa prijelaznih metala u zeolitima [Undergraduate thesis]. Osijek: Josip Juraj Strossmayer University of Osijek, Department of Chemistry; 2022 [cited 2025 February 13] Available at: https://urn.nsk.hr/urn:nbn:hr:182:722405

D. Šinjori, "Mehanokemijska sinteza kompleksa prijelaznih metala u zeolitima", Undergraduate thesis, Josip Juraj Strossmayer University of Osijek, Department of Chemistry, Osijek, 2022. Available at: https://urn.nsk.hr/urn:nbn:hr:182:722405

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Metadata
TitleMehanokemijska sinteza kompleksa prijelaznih metala u zeolitima
Title (english)Mechanochemical synthesis of transition metal complexes in zeolites
AuthorDamjan Šinjori
MentorAnamarija Stanković (mentor)
MentorAna Palčić (komentor)
MBZ: 305135
GranterJosip Juraj Strossmayer University of Osijek
Department of Chemistry
(Department of General, Inorganic and Physical Chemistry and Methodology of Chemistry)
Osijek
Defense date and country2022-09-19, Croatia
Scientific / art field,
discipline and subdiscipline		NATURAL SCIENCES
Chemistry
Inorganic Chemistry
Abstract
Zeoliti su aluminosilikati, klasa poroznih spojeva sa šupljinama i kanalima različitih veličina i oblika. Često se upotrebljavaju za pripremu inkluzijskih spojeva koji se mogu iskoristiti za razne primjene, kao što su kataliza, apsorpcija plinova te ionska izmjena. Kompleksni se spojevi mogu prirediti unutar šupljina zeolita otopinskom sintezom kako bi se utjecalo na njihova svojstva. Mehanokemija je grana kemije koja koristi mehaničku energiju za provedbu reakcija. Budući da se reakcije provode u krutom stanju, za njih nije potrebno koristiti velike količine otapala. To čini mehanokemiju jeftinijom, bržom i ekološki osvještenijom alternativom za klasičnu sintezu u otopini. Cilj ovog rada je mehanokemijski sintetizirati kompleksne spojeve nikla(II) i bakra(II) unutar zeolita Y bez korištenja otapala. Dobiveni produkti analizirani su IR spektroskopijom i difrakcijom rentgenskog zračenja u polikristalnom uzorku.
Abstract (english)
Zeolites are aluminosilicates, a class of porous compounds comprised of canals and cavities of different shapes and sizes. This makes them great candidates for preparation of inclusion compounds which have many uses, like reaction catalysis, gas absorption, ion-exchange etc. Complex coordination compounds can be synthesised inside the structure of a zeolite using solution synthesis methods to modify the properties of the material. Mechanochemistry is a branch of chemistry which uses mechanical energy to bring about a chemical reaction. Because those reactions are conducted in solid-state, no solvent is used which makes mechanochemistry a cheap, quick and eco-friendly alternative to classis solution synthesis. The goal of this research is to prepare transition metal complexes inside of zeolite Y’s crystal structure without the use of any solvents. Synthesis of nickel and copper cyanides was chosen for this purpose. The results were analysed by IR spectroscopy and powder X-ray diffraction.
Keywords
Keywords (english)
Languagecroatian
URN:NBNurn:nbn:hr:182:722405
Study programmeTitle: Chemistry
Study programme type: university
Study level: undergraduate
Academic / professional title: sveučilišni/a prvostupnik/prvostupnica (baccalaureus/baccalaurea) kemije (sveučilišni/a prvostupnik/prvostupnica (baccalaureus/baccalaurea) kemije)
Type of resourceText
File originBorn digital
Access conditionsOpen access
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Created on2022-11-02 08:46:47