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master's thesis
Priprava nanokristalnih jednostavnih oksidnih perovskita na bazi prijelaznih metala i lantanoida
2022. urn:nbn:hr:182:326492
Basara, Roberto
Josip Juraj Strossmayer University of Osijek
Department of Chemistry
Department of Analytical, Organic and Applied Chemistry

Cite this document

Basara, R. (2022). Priprava nanokristalnih jednostavnih oksidnih perovskita na bazi prijelaznih metala i lantanoida (Master's thesis). Osijek: Josip Juraj Strossmayer University of Osijek, Department of Chemistry. Retrieved from https://urn.nsk.hr/urn:nbn:hr:182:326492

Basara, Roberto. "Priprava nanokristalnih jednostavnih oksidnih perovskita na bazi prijelaznih metala i lantanoida." Master's thesis, Josip Juraj Strossmayer University of Osijek, Department of Chemistry, 2022. https://urn.nsk.hr/urn:nbn:hr:182:326492

Basara, Roberto. "Priprava nanokristalnih jednostavnih oksidnih perovskita na bazi prijelaznih metala i lantanoida." Master's thesis, Josip Juraj Strossmayer University of Osijek, Department of Chemistry, 2022. https://urn.nsk.hr/urn:nbn:hr:182:326492

Basara, R. (2022). 'Priprava nanokristalnih jednostavnih oksidnih perovskita na bazi prijelaznih metala i lantanoida', Master's thesis, Josip Juraj Strossmayer University of Osijek, Department of Chemistry, accessed 26 October 2024, https://urn.nsk.hr/urn:nbn:hr:182:326492

Basara R. Priprava nanokristalnih jednostavnih oksidnih perovskita na bazi prijelaznih metala i lantanoida [Master's thesis]. Osijek: Josip Juraj Strossmayer University of Osijek, Department of Chemistry; 2022 [cited 2024 October 26] Available at: https://urn.nsk.hr/urn:nbn:hr:182:326492

R. Basara, "Priprava nanokristalnih jednostavnih oksidnih perovskita na bazi prijelaznih metala i lantanoida", Master's thesis, Josip Juraj Strossmayer University of Osijek, Department of Chemistry, Osijek, 2022. Available at: https://urn.nsk.hr/urn:nbn:hr:182:326492

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Metadata
TitlePriprava nanokristalnih jednostavnih oksidnih perovskita na bazi prijelaznih metala i lantanoida
Title (english)Synthesis of simple nanocrystalline oxide-based perovskites comprising transition metals and lanthanides
AuthorRoberto Basara
MentorIgor Đerđ (mentor)
MentorJelena Kojčinović (pomoć pri izradi, neposredni voditelj)
Committee memberBerislav Marković (predsjednik povjerenstva)
Committee memberIgor Đerđ (član povjerenstva)
Committee memberElvira Kovač-Andrić (član povjerenstva)
GranterJosip Juraj Strossmayer University of Osijek
Department of Chemistry
(Department of Analytical, Organic and Applied Chemistry)
Osijek
Defense date and country2022-09-20, Croatia
Scientific / art field,
discipline and subdiscipline		NATURAL SCIENCES
Chemistry
Applied Chemistry
Abstract
Kako je u današnje vrijeme porasla potreba za novim materijalima s velikim izborom svojstava, istraživanje perovskita uvelike je poraslo. Zbog velike mogućnosti dopiranja ovih spojeva, perovskiti su se pokazali kao odlični kandidati za veliki broj novih tehnologija. U ovom diplomskom radu sintetizirani su nanokristalni oksidni perovskiti na bazi prijelaznih metala i lantanoida. Cilj uvođenja novih elemenata u sustav je povećati konfiguracijsku entropiju sustava kako bi se povećala njihova stabilnost te kako bi spojevi dobili nova svojstva. Svi navedeni perovskiti sintetizirani su modificiranom citratnom sol–gel metodom pri istim uvjetima, te su svi spojevi prošli jedan korak kalcinacije pri 600 °C u struji zraka s temperaturom zagrijavanja od 2 °C/min. Dobivani spojevi zatim su okarakterizirani rentgenskom difrakcijom na prahu (PXRD), termogravimetrijskom analizom (TGA/DSC), UV/VIS spektroskopijom i analizom specifične površine i eventualne poroznosti Brunauer–Emmett–Teller (BET) metodom.
Abstract (english)
As the need for new materials with a wide variety of properties has increased nowadays, perovskite research has grown greatly. Due to the high possibility of doping these compounds, perovskites have proven to be excellent candidates for a large number of new technologies. In this thesis, nanocrystalline oxide perovskites based on transition metals and lanthanides were synthesized. The goal of introducing new elements into the system is to increase the configurational entropy of the system in order to increase their stability and to give the compounds new properties. All the mentioned perovskites were synthesized by a modified citrate sol-gel method under the same conditions, and all compounds underwent one step of calcination at 600 °C in an air flow with a heating temperature of 2 °C/min. The obtained compounds were further characterized by the X-ray powder diffraction (PXRD), thermogravimetric analysis (TGA/DSC), UV/VIS spectroscopy, and Brunauer–Emmett–Teller (BET) analysis.
Keywords
Keywords (english)
Languagecroatian
URN:NBNurn:nbn:hr:182:326492
ProjectNumber: PZS-2019-02-2467
Title: Istraživanje utjecaja metalnih promotora rijetkih zemalja i stupnja uređenja na redoks svojstva sustava CeO2 - ZrO2
Title: The study of the role of rare earth metal promoters and ordering on the redox properties of CeO2 - ZrO2 system
Acronym: SREMPOREPROCEZIS
Leader: Igor Đerđ
Jurisdiction: Croatia
Funder: HRZZ
Funding stream: PZS
Study programmeTitle: Graduate University Study of Chemistry; research program; specializations in: Research program
Course: Research program
Study programme type: university
Study level: graduate
Academic / professional title: magistar/magistra kemije (magistar/magistra kemije)
Type of resourceText
File originBorn digital
Access conditionsOpen access
Terms of useLicence In copyright icon
Created on2022-11-02 12:07:35