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master's thesis
Sinteza metalo-organskih mreža lantanoida i njihovih derivata
2023. urn:nbn:hr:182:086322
Šilješ, Tomislav
Josip Juraj Strossmayer University of Osijek
Department of Chemistry
Department of Analytical, Organic and Applied Chemistry

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Šilješ, T. (2023). Sinteza metalo-organskih mreža lantanoida i njihovih derivata (Master's thesis). Osijek: Josip Juraj Strossmayer University of Osijek, Department of Chemistry. Retrieved from https://urn.nsk.hr/urn:nbn:hr:182:086322

Šilješ, Tomislav. "Sinteza metalo-organskih mreža lantanoida i njihovih derivata." Master's thesis, Josip Juraj Strossmayer University of Osijek, Department of Chemistry, 2023. https://urn.nsk.hr/urn:nbn:hr:182:086322

Šilješ, Tomislav. "Sinteza metalo-organskih mreža lantanoida i njihovih derivata." Master's thesis, Josip Juraj Strossmayer University of Osijek, Department of Chemistry, 2023. https://urn.nsk.hr/urn:nbn:hr:182:086322

Šilješ, T. (2023). 'Sinteza metalo-organskih mreža lantanoida i njihovih derivata', Master's thesis, Josip Juraj Strossmayer University of Osijek, Department of Chemistry, accessed 18 November 2024, https://urn.nsk.hr/urn:nbn:hr:182:086322

Šilješ T. Sinteza metalo-organskih mreža lantanoida i njihovih derivata [Master's thesis]. Osijek: Josip Juraj Strossmayer University of Osijek, Department of Chemistry; 2023 [cited 2024 November 18] Available at: https://urn.nsk.hr/urn:nbn:hr:182:086322

T. Šilješ, "Sinteza metalo-organskih mreža lantanoida i njihovih derivata", Master's thesis, Josip Juraj Strossmayer University of Osijek, Department of Chemistry, Osijek, 2023. Available at: https://urn.nsk.hr/urn:nbn:hr:182:086322

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Metadata
TitleSinteza metalo-organskih mreža lantanoida i njihovih derivata
Title (english)Synthesis of lanthanide metal-organic frameworks and their derivates
AuthorTomislav Šilješ
MentorIgor Đerđ (mentor)
Committee memberElvira Kovač-Andrić (predsjednik povjerenstva)
Committee memberIgor Đerđ (član povjerenstva)
Committee memberAnamarija Stanković (član povjerenstva)
GranterJosip Juraj Strossmayer University of Osijek
Department of Chemistry
(Department of Analytical, Organic and Applied Chemistry)
Osijek
Defense date and country2023-09-11, Croatia
Scientific / art field,
discipline and subdiscipline		NATURAL SCIENCES
Chemistry
Applied Chemistry
Abstract
Solvotermalnom sintezom u smjesi otapala N, N – dimetilformamida (DMF) i vode sintetizirane su metalo-organske mreže (MOF) na osnovi lantanoida, itrija i cirkonija s jantarnom kiselinom. Cilj ovog istraživanja je dobiti jednofazne MOF-ove s jednim ili više metala u strukturi kako bi nastali visokoentropijski spojevi te ispitati koji derivati nastaju termičkom razgradnjom istih. Pripremljeni spojevi su okarakterizirani rentgenskom difrakcijom u prahu (PXRD), termogravimetrijskom analizom s razlikovnom pretražnom kalorimetrijom (TGA/DSC), pretražnom elektronskom mikroskopijom s energijski razlučujućom rentgenskom spektroskopijom (SEM-EDS), analizirana im je specifična površina i veličina pora pomoću analizatora specifične površine i veličine pora, te je odabranim spojevima ispitana katalitička aktivnost na fotokatalitičku hidrogenaciju CO2.
Abstract (english)
Metal-organic networks (MOFs) based on lanthanides, yttrium and zirconium with succinic acid were synthesized by solvothermal synthesis in the solvent mixture of N, N – dimethylformamide (DMF) and water. The goal of this research is to synthesize single-phase MOFs with one or more metals in the structure in order to create high-entropy compounds and to investigate the type of derivates that are obtained by their thermal degradation. Obtained compounds were characterized by powder X-ray diffraction (PXRD), thermogravimetric analysis with differential scanning calorimetry (TGA/DSC), scanning electron microscopy with energy dispersive X-ray spectroscopy (SEM-EDS), while their specific surface areas and pore sizes were investigated using surface area and pore size analyzer, and the catalytic activity of selected compounds was examined towards the photocatalytic hydrogenation of CO2.
Keywords
Keywords (english)
Languagecroatian
URN:NBNurn:nbn:hr:182:086322
Study programmeTitle: University Graduate Study of Chemistry; Research Program; specializations in: Research Program
Course: Research Program
Study programme type: university
Study level: graduate
Academic / professional title: sveučilišni/a magistar/magistra kemije (sveučilišni/a magistar/magistra kemije)
Type of resourceText
File originBorn digital
Access conditionsOpen access
Terms of useLicence In copyright icon
Created on2023-11-06 09:30:39