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master's thesis
Sinteza makrocikličkih Schiffovih baza iz diketona i diamina
2014. urn:nbn:hr:182:772139
Babić, Hrvoje
Josip Juraj Strossmayer University of Osijek
Department of Chemistry

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Babić, H. (2014). Sinteza makrocikličkih Schiffovih baza iz diketona i diamina (Master's thesis). Osijek: Josip Juraj Strossmayer University of Osijek, Department of Chemistry. Retrieved from https://urn.nsk.hr/urn:nbn:hr:182:772139

Babić, Hrvoje. "Sinteza makrocikličkih Schiffovih baza iz diketona i diamina." Master's thesis, Josip Juraj Strossmayer University of Osijek, Department of Chemistry, 2014. https://urn.nsk.hr/urn:nbn:hr:182:772139

Babić, Hrvoje. "Sinteza makrocikličkih Schiffovih baza iz diketona i diamina." Master's thesis, Josip Juraj Strossmayer University of Osijek, Department of Chemistry, 2014. https://urn.nsk.hr/urn:nbn:hr:182:772139

Babić, H. (2014). 'Sinteza makrocikličkih Schiffovih baza iz diketona i diamina', Master's thesis, Josip Juraj Strossmayer University of Osijek, Department of Chemistry, accessed 18 November 2024, https://urn.nsk.hr/urn:nbn:hr:182:772139

Babić H. Sinteza makrocikličkih Schiffovih baza iz diketona i diamina [Master's thesis]. Osijek: Josip Juraj Strossmayer University of Osijek, Department of Chemistry; 2014 [cited 2024 November 18] Available at: https://urn.nsk.hr/urn:nbn:hr:182:772139

H. Babić, "Sinteza makrocikličkih Schiffovih baza iz diketona i diamina", Master's thesis, Josip Juraj Strossmayer University of Osijek, Department of Chemistry, Osijek, 2014. Available at: https://urn.nsk.hr/urn:nbn:hr:182:772139

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Metadata
TitleSinteza makrocikličkih Schiffovih baza iz diketona i diamina
Title (english)Synthesis of Macrocyclic Schiff Bases from Diketones and Diamines
AuthorHrvoje Babić
MentorBerislav Marković (mentor)
MentorTomislav Balić (komentor)
Committee memberIvan Vicković (predsjednik povjerenstva)
Committee memberBerislav Marković (član povjerenstva)
Committee memberDajana Gašo-Sokač (član povjerenstva)
Committee memberTomislav Balić (član povjerenstva)
GranterJosip Juraj Strossmayer University of Osijek
Department of Chemistry
Osijek
Defense date and country2014-11-13, Croatia
Scientific / art field,
discipline and subdiscipline		NATURAL SCIENCES
Chemistry
Abstract
Makrocikli su molekule cikličke strukture od najmanje devet atoma u prstenu. Makrocikli nalaze primjenu u širokom području istraživanja. Makrocikličke Schiffove baze čine dio makrocikličke kemije koji je vrlo popularan zbog njihove jednostavne primjene. U ovome radu opisan je pokušaj dobivanja novih makrocikličkih Schiffovih baza iz diketona i diamina. Pomoću templatne sinteze dobivene su Schiffove baze iz komercijalno dostupnih reaktanata. Dobiveni su i polioksa makrocikli iz priređenih diketona i dialdehida trivijalnog naziva Chalcon-i. Svi dobiveni produkti karakterizirani su FTIR i TG/DSC metodom. Rad također sadržava i metodički dio u kojem je opisana priprema za nastavni sat na temu "Aldehidi i ketoni" za srednju školu, uključujući i radne listiće za pripadajuće pokuse.
Abstract (english)
Macrocycles are circular shape molecules consisting of at least nine atoms in a ring. They can be applied in a wide area of research. Macrocyclic Schiff bases are a very popular part of macrocyclic chemistry since they can be easily applied and their synthesis is rather simple due to affordable prices of reagents. This paper describes an attempt of synthesis of novel macrocyclic Schiff bases from diketones and diamines. Using template synthesis, Schiff bases were obtained from commercialy available reagents. Polyoxa macrocycles, trivialy named chalcones, were also obtained from prepared diketones and dialdehydes. Obtained products were characterised with FTIR and TGA-DSC methods of analysis. In the teaching part of the paper a preparation lecture on aldehydes and ketones for the high school chemistry class is proposed. The lecture also includes relevant experiments and handouts.
Keywords
Keywords (english)
Languagecroatian
URN:NBNurn:nbn:hr:182:772139
Study programmeTitle: Chemistry
Study programme type: university
Study level: graduate
Academic / professional title: magistar/magistra edukacije kemije (magistar/magistra edukacije kemije)
Type of resourceText
File originBorn digital
Access conditionsOpen access
Terms of useLicence In copyright icon
Created on2016-07-18 08:54:14